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[학술저널]

  • 학술저널

La Ode Rusman(Universitas Gadjah Mada) Amjad Tri Puspitasari(Universitas Gadjah Mada) Edi Suharyadi(Universitas Gadjah Mada) Takeshi Kato(Nagoya University) Satoshi Iwata(Nagoya University)

DOI : 10.4283/JMAG.2019.24.1.149

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초록

Zinc-doped cobalt ferrite magnetic nanoparticles (CoZnFe₂O₄) with silica encapsulation have been successfully synthesized by using coprecipitation method. The concentration of silica was varied by 0 %, 5 %, 10 %, 15 %, 20 %, 30 % and 50 % of weight. The XRD spectra show that all samples have the character of the main spinel diffraction peaks (2θ) attributed to the (220), (311), (400), (422), and (511) planes. The FTIR analysis shows that the intrinsic stretching vibrations of metal-oxygen at the frequency range of 393 ㎝−1 - 401 ㎝−1 and 470 ㎝−1 - 563 ㎝−1 were found at octahedral and tetrahedral sublattices, respectively. The unencapsulated CoZnFe₂O₄ nanoparticle has coercivity (Hc) and maximum magnetization (M) of 251 Oe and 29.0 emu/gram, respectively. The coercivity value of the encapsulated nanoparticles increases up to 853 Oe with the increase of silica concentration, while the maximum magnetization decreases to 24.2 emu/gram.

목차

1. Introduction
2. Experimental Method
3. Results and Discussion
4. Conclusion
References

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