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학술연구/단체지원/교육 등 연구자 활동을 지속하도록 DBpia가 지원하고 있어요.
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연구자들이 자신의 연구와 전문성을 널리 알리고, 새로운 협력의 기회를 만들 수 있는 네트워킹 공간이에요.
초록· 키워드
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Two thickness measurement methods using an electron energy loss spectroscopy (EELS) and 10a convergent beam electron diffraction (CBED) were compared in an Fe-18Mn-0.7C alloy. The thin foil specimen was firstly tilted to satisfy 10a two-beam condition. Low loss spectra of EELS and CBED patterns were acquired in scanning transmission electron microscopy (STEM) and TEM-CBED modes under the two-beam condition. The log-ratio method was used for measuring the thin foil thickness. Kossel-Möllenstedt (K-M) fringe of the 131 diffracted disk of austenite was analyzed to evaluate the thickness. The results prove the good coherency between both methods in the thickness range of 72 ~ 113 nm with a difference of less than 5%.
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참고문헌 (13)
참고문헌 신청
S. M. Allen / 1981 / Foil thickness measurements from convergent-beam diffraction patterns / Phil. Mag. A 43:325~335
J. E. Bailey / 1960 / The dislocation distribution, flow stress, and stored energy in cold-worked polycrystalline silver / Phil. Mag 5:485~497
F. Delmas / 2004 / Quantitative TEM study of the precipitation microstructure in aluminium alloy Al (MgSiCu) 6056 T6 / Mater. Sci. Eng. A 373:80~89
T. Dorin / 2015 / Size distribution and volume fraction of T1 phase precipitates from TEM images: Direct measurements and related correction / Micron 78:19~27
R. F. Egerton / 1996 / Electron Energy-Loss Spectroscopy in the Electron Microscope / Plenum press
J. E. Bailey / 1960 / The dislocation distribution, flow stress, and stored energy in cold-worked polycrystalline silver / Phil. Mag 5:485~497
F. Delmas / 2004 / Quantitative TEM study of the precipitation microstructure in aluminium alloy Al (MgSiCu) 6056 T6 / Mater. Sci. Eng. A 373:80~89
T. Dorin / 2015 / Size distribution and volume fraction of T1 phase precipitates from TEM images: Direct measurements and related correction / Micron 78:19~27
R. F. Egerton / 1996 / Electron Energy-Loss Spectroscopy in the Electron Microscope / Plenum press
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