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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 저널정보
- 한국고분자학회 폴리머 폴리머 제45권 제1호
- 발행연도
- 2021.1
- 수록면
- 101 - 112 (12page)
- DOI
- 10.7317/pk.2021.45.1.101
이용수
초록· 키워드
오류제보하기
The solid electrolyte membrane for a hydrogen-oxygen fuel cell was prepared and investigated from the potential of sulfonated poly(ether ether ketone) (SPEEK) embedded together with montmorillonite (MMT). Acid hydrophilized poly(ether ether ketone) (PEEK) and MMT with varying sulfonation levels of 25-70% prepared through solvent casting were investigated for their performance. The nuclear magnetic resonance (1H NMR) spectra at 7.5 ppm affirmed the occurrence of sulfonation reaction, and its degree was studied by both 1H NMR and titration method. The reaction time was varied to achieve sulfonation levels from 25 to 70%. The effect of incorporation of pristine and sulfonated MMT into SPEEK was examined. The membranes, prepared using solvent casting technique, were involved for water uptake over the wide range of temperature, thermal stability, and proton conductivity measurements. The cross-sectional surface arrangement of the membrane and clay dispersion was deliberated using SEM. The proton exchange membrane fuel cell (PEMFC) single cell’s tests revealed that sulfonated PEEK membrane demonstrated service performance comparable to that of Nafion, as validated using MATLAB software.
목차
Abstract
Introduction
Experimental
Results and Discussion
Conclusions
References
참고문헌 (39)
참고문헌 신청
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Appleby, A. J. Recent Developments and Applications of the 2021 Polymer Fuel Cell. Phil. Trans. R. Soc. Lond. A 1996, 354, 1681-1693.
Shoesmith, J. P.; Collins, R. D.; Oakley, M. J.; Stevenson, D. K. J. Status of Solid Polymer Fuel Cell System Development. Power Sources 1994, 49, 129-142.
Gao, Y.; Robertson, G. P.; Guiver, M. D.; Mikhailenko, S. D.; Li, X.; Kaliaguine, S. Synthesis of Poly(arylene ether ether ketone ketone) Copolymers Containing Pendant Sulfonic Acid Groups Bonded to Naphthalene as Proton Exchange Membrane Materials. Macromolecules 2004, 37, 6748-6754.
Savadogo, O. Emerging Membranes for Electrochemical Systems: (I) Solid Polymer Electrolyte Membranes for Fuel Cell Systems. J. New. Mater. Electrochem. Syst. 1998, 1, 47-66.
Appleby, A. J. Recent Developments and Applications of the 2021 Polymer Fuel Cell. Phil. Trans. R. Soc. Lond. A 1996, 354, 1681-1693.
Shoesmith, J. P.; Collins, R. D.; Oakley, M. J.; Stevenson, D. K. J. Status of Solid Polymer Fuel Cell System Development. Power Sources 1994, 49, 129-142.
Gao, Y.; Robertson, G. P.; Guiver, M. D.; Mikhailenko, S. D.; Li, X.; Kaliaguine, S. Synthesis of Poly(arylene ether ether ketone ketone) Copolymers Containing Pendant Sulfonic Acid Groups Bonded to Naphthalene as Proton Exchange Membrane Materials. Macromolecules 2004, 37, 6748-6754.
Savadogo, O. Emerging Membranes for Electrochemical Systems: (I) Solid Polymer Electrolyte Membranes for Fuel Cell Systems. J. New. Mater. Electrochem. Syst. 1998, 1, 47-66.
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