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논문 기본 정보
- 자료유형
- 학술저널
- 저자정보
- 발행연도
- 2014.10
- 수록면
- 475 - 481 (7page)
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Ammonia borane (NH₃BH₃), as a source material for energy generation and hydrogen storage, hasattracted growing interest due to its high hydrogen content. We have investigated the synthesis of ammonia borane from sodium borohydride (NaBH₄) and ammonium chloride (NH4Cl) utilizing a low-temperature process. Fromour results, we obtained a maximum synthetic yield of 98.2% of ammonia borane complex. The diammoniatediborane (DADB) was detected in about 5~10mol% with in the solid ammonia borane by solid-state <sup>11</sup>B-NMRanalysis. The synthesized solid ammonia borane products were studied to characterize hydrogen release uponthermal dehydrogenation.
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참고문헌 (11)
참고문헌 신청
P. Veeraraghavan / 2007 / Preparation of Ammonia Borane in High Yield and Purity, Methanolysis and Regeneration / Inorganic Chemistry 46(19):7810~7817
H. T. Hwang / 2012 / High and rapid hydrogen release from thermolysis of ammoia borane near PEM fuel cell operating temperature : Effect of quartz wool / J. Hydro. Energy 37:6764~6770
C. F. Lane / 2006 / Ammonia-Borane and Related N-B-H Compounds and Materials : Safety Aspects, Properties and Applications
D. J. Heldebrant / 2008 / Synthesis of ammonia borane for hydrogen storage application / Energy Environ. Sci 1:156~160
S. G. Shore / 1964 / Large Scale Synthesis of H2B(NH3)2+BH4-and H3NBH3 / Inorg. Chem. 3(6):914~915
H. T. Hwang / 2012 / High and rapid hydrogen release from thermolysis of ammoia borane near PEM fuel cell operating temperature : Effect of quartz wool / J. Hydro. Energy 37:6764~6770
C. F. Lane / 2006 / Ammonia-Borane and Related N-B-H Compounds and Materials : Safety Aspects, Properties and Applications
D. J. Heldebrant / 2008 / Synthesis of ammonia borane for hydrogen storage application / Energy Environ. Sci 1:156~160
S. G. Shore / 1964 / Large Scale Synthesis of H2B(NH3)2+BH4-and H3NBH3 / Inorg. Chem. 3(6):914~915
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