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논문 기본 정보

자료유형
학술저널
저자정보
Li-li Wang (Shaanxi University of Science & Technology)
저널정보
한양대학교 세라믹공정연구센터 Journal of Ceramic Processing Research Journal of Ceramic Processing Research 제18권 제6호
발행연도
2017.6
수록면
457 - 462 (6page)
DOI
http://dx.doi.org/

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Polystyrene colloidal template was prepared by evaporation deposition method with as-prepared polystyrene microsphereswith the size of 340±10nm as raw material and inverse opal zirconia was fabricated by colloidal crystal-templating method. The optimal process of preparation of polystyrene colloidal template and inverse opal zirconia were deeply studied viaorthogonal experiment design and range date processing. The factors, which affect the morphology of polystyrene templateand inverse opal zirconia, and the corresponding values were considered, respectively and the primary and secondary orderof factors were also determined. The results showed that the optimal process of preparation of polystyrene colloidal templatewas that self-assembly temperature was 55 oC, emulsion height was 1.5 cm, emulsion consistence kept 4.0% and containerdiameter was Φ6.0 cm. It also found that the as-prepared polystyrene template showed bright green color and the betterpolystyrene template structure was, the brighter green color can be obtained. The optimal process of preparation of inverseopal zirconia was that impregnation time was once, mass ratio of polystyrene template and precursor kept 1 : 15, precursorratio of zirconium acetate and methanol kept 1 : 1 and calcination temperature was 450 oC.

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